反应条件
1.1: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / tetrachloromethane / 14 h / |Reflux; |Inert atmosphere 2.1: ammonia / tetrahydrofuran / 20 °C 3.1: tertiary amine / dichloromethane / 0.08 h / |Cooling 3.2: 1.17 h / 0 - 20 °C 4.1: trichlorophosphate / toluene / 2 h / |Reflux View Scheme
参考文献
Olszewska, Teresa; Gajewska, Ewa P.; Milewska, Maria J.
Tetrahedron, 2013 , vol. 69, # 2 p. 474 - 480
