3-溴-2'-甲氧基-2-联苯醇合成路线 (共 4 条)
反应条件
potassium carbonate in acetone Heating;
参考文献
Baret; Beguin; Gaude; Gellon; Mourral; Pierre; Serratrice; Favier
Tetrahedron, 1994 , vol. 50, # 7 p. 2077 - 2094
反应条件
1: 87 percent / K2CO3 / acetone / Heating 2: 94 percent / Br2, t-butylamine / toluene; CH2Cl2 / -70 °C 3: 87 percent / K2CO3 / acetone / Heating View Scheme
参考文献
Baret; Beguin; Gaude; Gellon; Mourral; Pierre; Serratrice; Favier
Tetrahedron, 1994 , vol. 50, # 7 p. 2077 - 2094
反应条件
1: 94 percent / Br2, t-butylamine / toluene; CH2Cl2 / -70 °C 2: 87 percent / K2CO3 / acetone / Heating View Scheme
参考文献
Baret; Beguin; Gaude; Gellon; Mourral; Pierre; Serratrice; Favier
Tetrahedron, 1994 , vol. 50, # 7 p. 2077 - 2094
反应条件
sec.-butyllithium 1.) ether, hexane, -40 deg C, 20 min; 2.) 3 h, -40 deg C;
参考文献
Baret; Beguin; Gaude; Gellon; Mourral; Pierre; Serratrice; Favier
Tetrahedron, 1994 , vol. 50, # 7 p. 2077 - 2094