反应条件
1.1: tetrahydrofuran / 0 °C / |Inert atmosphere 1.2: |Inert atmosphere 2.1: pyridinium chlorochromate / dichloromethane / 4 h / 0 °C / |Inert atmosphere 3.1: MgBr2(Et2O) / diethyl ether / 2 h / 20 °C 4.1: sodium hydroxide; DCN; biphenyl / acetonitrile; water / 6 h / 20 °C / |Inert atmosphere; |UV-irradiation View Scheme
参考文献
Nishikawa, Keisuke; Yoshimi, Yasuharu; Maeda, Kousuke; Morita, Toshio; Takahashi, Ichiro; Itou, Tatsuya; Inagaki, Sho; Hatanaka, Minoru
Journal of Organic Chemistry, 2013 , vol. 78, # 2 p. 582 - 589