3,5-二氯-4-[3-(2,6-二氯-4-羟基苯氧基)-2,5-二甲氧基苯氧基]苯酚合成路线 (共 13 条)
反应条件
1: satd. aq. Na2S2O4 2: 88 percent / K2CO3 / acetone / 6 h / 45 °C 3: 72 percent / CF3COOH / CH2Cl2 / 8 h View Scheme
参考文献
Reddy, K. Laxma; Vittal
Synthetic Communications, 1997 , vol. 27, # 1 p. 107 - 118
反应条件
1: 88 percent / K2CO3 / acetone / 6 h / 45 °C 2: 72 percent / CF3COOH / CH2Cl2 / 8 h View Scheme
参考文献
Reddy, K. Laxma; Vittal
Synthetic Communications, 1997 , vol. 27, # 1 p. 107 - 118
反应条件
copper(I) oxide; sulfuric acid; water; copper(II) nitrate; sodium nitrite 1.) 0 - 5 deg C, 5 min, 2.) RT, 30 min; Yield given. Multistep reaction;
参考文献
Takahashi; Agatsuma; Matsuda; Ohta; Nunozawa; Endo; Nozoe
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 12 p. 3185 - 3188