3-(N-苯基-N-甲基)氨基丙烯醛合成路线 （共 18 条）
反应条件
in 1,4-dioxane T=20 - 25°C; Product distribution / selectivity;
参考文献
RANBAXY LABORATORIES LIMITED
Patent: WO2006/90256 A1, 2006 ;
Location in patent: Page/Page column 11-12 ;
反应条件
gold nanoparticles supported on manganese-oxide-based octahedral molecular sieves; air in tetrahydrofuran; water T=50°C; P=760.051 Torr; 8 h;
参考文献
Jin, Xiongjie; Yamaguchi, Kazuya; Mizuno, Noritaka
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 455 - 458
Angew. Chem., 2014 , vol. 126, # 2 p. 465 - 468,4
反应条件
1: With oxalyl dichloride in acetonitrile T=-10 - 20°C; 2 h; Inert atmosphere; 2: With water; sodium carbonate in toluene; acetonitrile T=0 - 22°C; 1 h; Inert atmosphere;
参考文献
Zacharia, James T.; Tanaka, Takanori; Hayashi, Masahiko
Journal of Organic Chemistry, 2010 , vol. 75, # 22 p. 7514 - 7518
反应条件
manganese(IV) oxide in benzene Ambient temperature;
参考文献
Blake, Alexander J.; McNab, Hamish; Monahan, Lilian C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 425 - 429
反应条件
(i) aq. TsOH, (ii) /BRN= 741982/; Multistep reaction;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 35, p. 3618 - 3627
反应条件
tetrahydrofuran; diethyl ether; benzene
参考文献
Jutz
Chemische Berichte, 1959 , vol. 92, p. 1983,1988
反应条件
diethyl ether; benzene
参考文献
Jutz
Chemische Berichte, 1958 , vol. 91, p. 1867,1876
反应条件
1: 3-(N-methyl-N-phenylamino)-2-propenal With trichlorophosphate in acetonitrile T=-5 - 7°C; 0.916667 h; Inert atmosphere; 2: 3-(4'-fluorophenyl)-1-(1'-methylethyl)-1H-indole in acetonitrile 3 h; RefluxInert atmosphere;
参考文献
Zacharia, James T.; Tanaka, Takanori; Hayashi, Masahiko
Journal of Organic Chemistry, 2010 , vol. 75, # 22 p. 7514 - 7518
反应条件
N-benzyl-N,N,N-triethylammonium chloride; sodium carbonate in benzene T=50°C; 20 h;
参考文献
Kryshtal', G.V.; Burshtein, K.Ya.; Kul'ganek, V.V.; Yanovskaya, L.A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 11 p. 2328 - 2334
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 11 p. 2541 - 2550
参考文献
Chemische Berichte, , vol. 91, p. 1867,1876
