methyl-magnesium iodide; ammonium chloride in chlorobenzene
(dry Ar); refluxed 6 h, CH3MgI added dropwise, refluxed 1 h, cooled (ice bath), quenched with a aq. soln. of NH4Cl; pptd. by addition of methanol to a Et2O-soln.;
参考文献
Atchekzai, Jean; Guilhon, Florence; Mongeot, Henri; Frange, Bernard
Inorganica Chimica Acta, 1992 , vol. 202, p. 49 - 52