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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-羟基吡啶
合成路线
（共 394 条）
142-08-5
2-羟基吡啶
+
100-51-6
苯甲醇
→
反应条件
1753-62-4
+
40864-08-2
2-(苄氧基)吡啶
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran Ambient temperature;
参考文献
Comins, Daniel L.; Jianhua, Gao
Tetrahedron Letters, 1994 , vol. 35, # 18 p. 2819 - 2822
142-08-5
2-羟基吡啶
+
100-44-7
苄基氯
→
反应条件
1753-62-4
+
40864-08-2
2-(苄氧基)吡啶
反应条件
1: 2-hydroxy-pyridine With n-butyllithium T=25°C; 0.5 h; Ionic liquidInert atmosphere; 2: benzyl chloride T=25°C; 5 h; Ionic liquidInert atmosphere; Reagent/catalystSolvent;
参考文献
Vavilina; Zicmanis; Mekss; Klavins
Chemistry of Heterocyclic Compounds, 2008 , vol. 44, # 5 p. 549 - 558
Khim. Geterotsikl. Soedin., 2008 , # 5 p. 699 - 710
142-08-5
2-羟基吡啶
+
100-44-7
苄基氯
→
反应条件
40864-08-2
2-(苄氧基)吡啶
反应条件
1: 2-hydroxy-pyridine With silver carbonate T=25°C; 0.5 h; Ionic liquidInert atmosphere; 2: benzyl chloride T=25°C; 5 h; Ionic liquidInert atmosphere;
参考文献
Vavilina; Zicmanis; Mekss; Klavins
Chemistry of Heterocyclic Compounds, 2008 , vol. 44, # 5 p. 549 - 558
Khim. Geterotsikl. Soedin., 2008 , # 5 p. 699 - 710
142-08-5
2-羟基吡啶
+
100-44-7
苄基氯
→
反应条件
40864-08-2
2-(苄氧基)吡啶
+
108575-66-2
反应条件
potassium hydroxide in isopropyl alcohol T=50°C; Rate constant;
参考文献
Rajasekar, N.; Srinivasan, V. S.; Venkatasubramanian, N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 8 p. 800 - 802
142-08-5
2-羟基吡啶
+
100-39-0
溴化苄
→
反应条件
1753-62-4
+
40864-08-2
2-(苄氧基)吡啶
反应条件
potassium hydroxide; Aliquat 1 h; Ambient temperatureother alkyl halides; var. mole ratio of 2-pyridone :benzyl bromide : base; var. reaction time; Product distribution;
参考文献
Collina, Gianni; Forlani, Luciano; Mezzina, Elisabetta; Sintoni, Marina; Todesco, Paolo E.
Gazzetta Chimica Italiana, 1987 , vol. 117, # 5 p. 281 - 286
142-08-5
2-羟基吡啶
+
106-95-6
3-溴丙烯
→
反应条件
1753-62-4
+
40864-08-2
2-(苄氧基)吡啶
反应条件
silver carbonate in pentane 24 h; Ambient temperaturefurther alkyl halides, bases, solvents, times and temperatures; Product distribution;
参考文献
Collina, Gianni; Forlani, Luciano; Mezzina, Elisabetta; Sintoni, Marina; Todesco, Paolo E.
Gazzetta Chimica Italiana, 1987 , vol. 117, # 5 p. 281 - 286
142-08-5
2-羟基吡啶
+
6165-68-0
2-噻吩硼酸
→
反应条件
3319-99-1
2-(2-噻吩基)吡啶
反应条件
1: 2-hydroxy-pyridine With potassium carbonate; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate in 1,4-dioxane T=100°C; 3 h; Inert atmosphere; 2: dihydroxy-thien-2-ylborane With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane; water T=100°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Li, Shui-Ming; Huang, Jie; Chen, Guo-Jun; Han, Fu-She
Chemical Communications, 2011 , vol. 47, # 48 p. 12840 - 12842
142-08-5
2-羟基吡啶
→
反应条件
4214-79-3
5-氯-2-羟基吡啶
反应条件
sodium hypochlorite in dichloromethane Ambient temperature1.) 30 s 2.) 24 h;
参考文献
Katritzky, Alan R.; Khan, Ghulam R.; Leahy, David E.; Rosa, Michael De
Journal of Organic Chemistry, 1984 , vol. 49, # 25 p. 4784 - 4786
142-08-5
2-羟基吡啶
+
3058-39-7
4-碘氰基苯
→
反应条件
444002-96-4
4-(2-氧代-1(2H)-吡啶基)苯腈
反应条件
copper(l) iodide; 8-hydroxy-quinoline; caesium carbonate in dimethyl sulfoxide T=120°C;
参考文献
MILLENNIUM PHARMACEUTICALS, INC.
Patent: WO2006/2099 A2, 2006 ;
Location in patent: Page/Page column 193-194 ;
WO 2006/002099 A2
142-08-5
2-羟基吡啶
→
反应条件
444002-96-4
4-(2-氧代-1(2H)-吡啶基)苯腈
反应条件
copper(l) iodide; potassium carbonate; N,N'-dimethylcyclohexane-1,2-diamine in toluene 12 h; Heating;
参考文献
Wang, Po-Shih; Liang, Chih-Kai; Leung, Man-Kit
Tetrahedron, 2005 , vol. 61, # 11 p. 2931 - 2939
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