反应条件
1: With potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide T=-50 - -20°C; Julia-Kocienski type gem-difluoroolefination; 3 h; Inert atmosphere; 2: With hydrogenchloride; water; ammonium chloride in tetrahydrofuran; N,N-dimethyl-formamide T=-40 - 20°C; Inert atmosphere;
参考文献
Zhao, Yanchuan; Huang, Weizhou; Zhu, Lingui; Hu, Jinbo
Organic Letters, 2010 , vol. 12, # 7 p. 1444 - 1447