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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-羟基吡啶
合成路线
（共 394 条）
142-08-5
2-羟基吡啶
+
87199-16-4
3-甲酰基苯硼酸
→
反应条件
85553-53-3
3-(2-吡啶基)苯甲醛
反应条件
1: 2-hydroxy-pyridine With potassium carbonate; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate in 1,4-dioxane T=100°C; 3 h; Inert atmosphere; 2: 3-formylphenyl-boronic acid With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane; water T=100°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Li, Shui-Ming; Huang, Jie; Chen, Guo-Jun; Han, Fu-She
Chemical Communications, 2011 , vol. 47, # 48 p. 12840 - 12842
142-08-5
2-羟基吡啶
+
1692-15-5
吡啶-4-硼酸
→
反应条件
581-47-5
2,4'-二吡啶
反应条件
1: 2-hydroxy-pyridine With potassium carbonate; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate in 1,4-dioxane T=100°C; 3 h; Inert atmosphere; 2: (pyridin-4-yl)boronic acid With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane; water T=100°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Li, Shui-Ming; Huang, Jie; Chen, Guo-Jun; Han, Fu-She
Chemical Communications, 2011 , vol. 47, # 48 p. 12840 - 12842
142-08-5
2-羟基吡啶
→
反应条件
5418-51-9
2-羟基-5-硝基吡啶
反应条件
sulfuric acid; nitric acid
参考文献
Tschitschibabin; Schapiro
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1921 , vol. 53, p. 235,237
Chem. Zentralbl., 1923 , vol. 94, # III p. 1025
142-08-5
2-羟基吡啶
+
1679-18-1
4-氯苯硼酸
→
反应条件
5969-83-5
2-(4-氯苯基)吡啶
反应条件
1: 2-hydroxy-pyridine With potassium carbonate; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate in 1,4-dioxane T=100°C; 3 h; Inert atmosphere; 2: (4-Chlorophenyl)-boronic acid With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane; water T=100°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Li, Shui-Ming; Huang, Jie; Chen, Guo-Jun; Han, Fu-She
Chemical Communications, 2011 , vol. 47, # 48 p. 12840 - 12842
142-08-5
2-羟基吡啶
+
74-88-4
甲基碘
→
反应条件
694-85-9
1-甲基-2-吡啶酮
反应条件
potassium carbonate
参考文献
De Saroj; Ghorai, Sujit K.; Mal, Dipakranjan
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1598 - 1604
142-08-5
2-羟基吡啶
+
1719-57-9
氯甲基二甲基氯硅烷
→
反应条件
694-85-9
1-甲基-2-吡啶酮
反应条件
1: With 1,1,1,3,3,3-hexamethyl-disilazane in acetonitrile Methylation; cyclization; Heating; 2: With cesium fluoride Ring cleavage; 48 h; Heating;
参考文献
Bassindale, Alan R.; Parker, David J.; Patel, Pravin; Taylor, Peter G.
Tetrahedron Letters, 2000 , vol. 41, # 25 p. 4933 - 4936
142-08-5
2-羟基吡啶
+
61985-23-7
(9ci)-1H-咪唑-1-羧酸甲酯
→
反应条件
694-85-9
1-甲基-2-吡啶酮
反应条件
in acetonitrile T=80°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Heller, Stephen T.; Sarpong, Richmond
Tetrahedron, 2011 , vol. 67, # 46 p. 8851 - 8859
142-08-5
2-羟基吡啶
+
1445-45-0
原乙酸三甲酯
→
反应条件
694-85-9
1-甲基-2-吡啶酮
反应条件
4 A molecular sieve; lithium iodide 2 h; Heating;
参考文献
Janin, Yves L.; Huel, Christiane; Flad, Genevieve; Thirot, Sylvie
European Journal of Organic Chemistry, 2002 , # 11 p. 1763 - 1769
142-08-5
2-羟基吡啶
+
4637-24-5
N,N-二甲基甲酰胺二甲基缩醛
→
反应条件
694-85-9
1-甲基-2-吡啶酮
反应条件
in toluene 3 h; Heating;
参考文献
Janin, Yves L.; Huel, Christiane; Flad, Genevieve; Thirot, Sylvie
European Journal of Organic Chemistry, 2002 , # 11 p. 1763 - 1769
142-08-5
2-羟基吡啶
+
74-88-4
甲基碘
→
反应条件
694-85-9
1-甲基-2-吡啶酮
+
1628-89-3
2-甲氧基吡啶
反应条件
potassium carbonate in N,N-dimethyl-formamide 24 h; Ambient temperature;
参考文献
Kuzuya, Masayuki; Mano, Ei-ichi; Adachi, Michihiro; Noguchi, Akihiro; Okuda, Takachiyo
Chemistry Letters, 1982 , p. 475 - 478
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