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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-羟基吡啶
合成路线
（共 394 条）
142-08-5
2-羟基吡啶
+
1396274-89-7
→
反应条件
69914-12-1
反应条件
1,3-bis-(diphenylphosphino)propane; tetrabutylammomium bromide; palladium diacetate; caesium carbonate in 1,4-dioxane T=120°C; Buchwald-Hartwig Coupling; 0.5 h; Microwave irradiationInert atmosphereSealed tube;
参考文献
Khader, K.K. Abdul; Sajith, Ayyiliath M.; Padusha, M. Syed Ali; Nagaswarupa; Muralidharan
New Journal of Chemistry, 2014 , vol. 38, # 3 p. 1294 - 1305
142-08-5
2-羟基吡啶
+
13271-49-3
5,5-二甲基-3-溴环己-2-烯酮
→
反应条件
69914-12-1
反应条件
palladium diacetate; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=120°C; Buchwald-Hartwig Coupling; Microwave irradiationInert atmosphereSealed tube;
参考文献
Khader, K.K. Abdul; Sajith, Ayyiliath M.; Padusha, M. Syed Ali; Nagaswarupa; Muralidharan
New Journal of Chemistry, 2014 , vol. 38, # 3 p. 1294 - 1305
142-08-5
2-羟基吡啶
+
1396274-84-2
→
反应条件
69914-13-2
反应条件
tetrabutylammomium bromide; palladium diacetate; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=120°C; Buchwald-Hartwig Coupling; 0.5 h; Microwave irradiationInert atmosphereSealed tube;
参考文献
Khader, K.K. Abdul; Sajith, Ayyiliath M.; Padusha, M. Syed Ali; Nagaswarupa; Muralidharan
New Journal of Chemistry, 2014 , vol. 38, # 3 p. 1294 - 1305
142-08-5
2-羟基吡啶
+
56671-81-9
3-溴环己-2-烯-1-酮
→
反应条件
69914-13-2
反应条件
palladium diacetate; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=120°C; Buchwald-Hartwig Coupling; Microwave irradiationInert atmosphereSealed tube;
参考文献
Khader, K.K. Abdul; Sajith, Ayyiliath M.; Padusha, M. Syed Ali; Nagaswarupa; Muralidharan
New Journal of Chemistry, 2014 , vol. 38, # 3 p. 1294 - 1305
142-08-5
2-羟基吡啶
+
96-09-3
氧化苯乙烯
→
反应条件
69914-21-2
反应条件
boron trifluoride diethyl etherate; cadmium (II) iodide in dichloromethane T=20°C; 6 h;
参考文献
Kocak, Ahmet; Kurbanli, Sultan; Malkondu, Sait
Synthetic Communications, 2007 , vol. 37, # 21 p. 3697 - 3708
142-08-5
2-羟基吡啶
+
696-62-8
4-碘苯甲醚
→
反应条件
725256-40-6
1-(4-甲氧基苯基)吡啶-2(1H)-酮
反应条件
copper(l) iodide; tetrabutyl-ammonium chloride; sodium hydride in N,N-dimethyl-formamide T=110°C; 12 h; Product distribution / selectivity;
参考文献
Zhang, Huiping; Chen, Bang-Chi; Zhao, Rulin
Patent: US2006/69260 A1, 2006 ;
Location in patent: Page/Page column 11 ;
142-08-5
2-羟基吡啶
+
104-92-7
4-溴苯甲醚
→
反应条件
725256-40-6
1-(4-甲氧基苯基)吡啶-2(1H)-酮
反应条件
potassium phosphate; N-methyl-2-(methylamino)ethylamine; copper(l) iodide in 1,4-dioxane T=110°C; 22 h;
参考文献
Li, Chun Sing; Dixon, Darryl D.
Tetrahedron Letters, 2004 , vol. 45, # 22 p. 4257 - 4260
142-08-5
2-羟基吡啶
→
反应条件
725256-40-6
1-(4-甲氧基苯基)吡啶-2(1H)-酮
反应条件
potassium tert-butylate in tetrahydrofuran 3 h; Heating;
参考文献
Ikegai, Kazuhiro; Nagata, Yuzo; Mukaiyama, Teruaki
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 5 p. 761 - 767
142-08-5
2-羟基吡啶
+
74-86-2
乙炔
→
反应条件
7379-71-7
1-乙烯基-2(1H)-吡啶酮
反应条件
1,4-dioxane; potassium hydroxide T=145 - 150°C; unter Druck;
参考文献
Afonin, A. V.; Andriyankov, M. A.; Pertsikov, B. Z.; Voronov, V. K.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 11 p. 2202 - 2204
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 11 p. 2451 - 2454
142-08-5
2-羟基吡啶
+
64-18-6
甲酸
→
反应条件
74885-84-0
反应条件
dicyclohexyl-carbodiimide in dichloromethane T=0°C; 2 h;
参考文献
Effenberger, Franz; Keil, Michael; Bessey, Eberhard
Chemische Berichte, 1980 , vol. 113, # 6 p. 2110 - 2119
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