2,5-二甲基-3-己炔-2,5-二醇合成路线 （共 93 条）
反应条件
1: TsOH
2: <PhCH2NEt3>Cl, aq. NaOH
3: Li / 2-methyl-propan-2-ol
View Scheme
参考文献
Dehmlow,S.S.; Dehmlow,E.V.
Justus Liebigs Annalen der Chemie, 1973 , p. 1753 - 1756
反应条件
1,3,4,6,7,8-hexahydro-1-methyl-2H-pyrimido{1,2-a}pyrimidine in acetonitrile
T=100°C; P=37503.8 Torr; 24 h; Autoclave;
参考文献
Ca', Nicola Della; Gabriele, Bartolo; Ruffolo, Giuseppe; Veltri, Lucia; Zanetta, Tito; Costa, Mirco
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 1 p. 133 - 146
反应条件
1,3,4,6,7,8-hexahydro-1-methyl-2H-pyrimido{1,2-a}pyrimidine
T=100°C; P=7500.75 Torr; 24 h; Autoclave;
参考文献
Ca', Nicola Della; Gabriele, Bartolo; Ruffolo, Giuseppe; Veltri, Lucia; Zanetta, Tito; Costa, Mirco
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 1 p. 133 - 146
反应条件
1,3,4,6,7,8-hexahydro-1-methyl-2H-pyrimido{1,2-a}pyrimidine
T=100°C; P=7500.75 Torr; 24 h; Autoclave;
参考文献
Ca', Nicola Della; Gabriele, Bartolo; Ruffolo, Giuseppe; Veltri, Lucia; Zanetta, Tito; Costa, Mirco
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 1 p. 133 - 146
反应条件
1,3,4,6,7,8-hexahydro-1-methyl-2H-pyrimido{1,2-a}pyrimidine
T=100°C; P=7500.75 Torr; 24 h; Autoclave;
参考文献
Ca', Nicola Della; Gabriele, Bartolo; Ruffolo, Giuseppe; Veltri, Lucia; Zanetta, Tito; Costa, Mirco
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 1 p. 133 - 146
反应条件
1,3,4,6,7,8-hexahydro-1-methyl-2H-pyrimido{1,2-a}pyrimidine
T=100°C; P=7500.75 Torr; 24 h; Autoclave;
参考文献
Ca', Nicola Della; Gabriele, Bartolo; Ruffolo, Giuseppe; Veltri, Lucia; Zanetta, Tito; Costa, Mirco
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 1 p. 133 - 146
反应条件
benzoic acid; hydroxytriphenylsilane; Vanadium catalyst
参考文献
Yates, Peter; Burke, Patrick Michael
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1695 - 1704
反应条件
sulfuric acid
1.) 50 deg C, 2 h; 2.) r.t., 2 d;
参考文献
Yates, Peter; Burke, Patrick Michael
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1695 - 1704
反应条件
sulfuric acid
T=50°C; 2 h;
参考文献
Yates, Peter; Burke, Patrick Michael
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1695 - 1704
参考文献
Krestinski; Bashenowa-Koslowskaja
Chemische Berichte, 1933 , vol. 66, p. 98
Zhurnal Obshchei Khimii, 1932 , vol. 2, p. 832
Full Text Show Details
Krestinski; Bashenowa-Koslowskaja
Zhurnal Obshchei Khimii, 1932 , vol. 2, p. 833
Chemische Berichte, 1933 , vol. 66, p. 98
