1: mono-methyl malonate potassium salt With triethylamine; magnesium chloride in acetonitrile
T=20°C; 3 h;
2: n-pentylcarbonyl chloride With triethylamine in acetonitrile
T=20°C; 20 h; Further stages.;
1: With pyridine in dichloromethane
T=0 - 20°C; 10957.5 h; Inert atmosphere;
2: With methanol
3.5 h; Reflux;
参考文献
Case-Green, Stephen C.; Davies, Stephen G.; Roberts, Paul M.; Russell, Angela J.; Thomson, James E.
Tetrahedron Asymmetry, 2008 , vol. 19, # 22 p. 2620 - 2631
Yakhontov,L.N. et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1970 , vol. 6, p. 1444 - 1447
Khimiya Geterotsiklicheskikh Soedinenii, 1970 , vol. 6, p. 1546 - 1549
