反应条件
1: water-d2; 10 platinum on carbon; NaOD / 144 h / 220 °C 2: N,N-dimethyl-formamide; thionyl chloride / dichloromethane / 5 h / 50 °C 3: ammonium hydroxide / acetonitrile / 2 h / 0 - 20 °C 4: lithium aluminium deuteride / tetrahydrofuran / 12 h / 70 °C / |Cooling; |Inert atmosphere View Scheme
参考文献
Yepuri, Nageshwar R.; Jamieson, Scott A.; Darwish, Tamim A.; Rawal, Aditya; Hook, James M.; Thordarson, Pall; Holden, Peter J.; James, Michael
Tetrahedron Letters, 2013 , vol. 54, # 20 p. 2538 - 2541
