(E,E)-2,4-己二烯醛合成路线 (共 87 条)
反应条件
oxygen; Pd561phen60(OAc)180 in acetic acid T=60°C; 2 h;
参考文献
Kaneda, Kiyotomi; Fujie, Yoko; Ebitani, Kohki
Tetrahedron Letters, 1997 , vol. 38, # 52 p. 9023 - 9026
反应条件
water; sodium acetate; acetic acid T=95°C; stereoselective reaction;
参考文献
Tetrahedron, , vol. 67, # 1 p. 173 - 178
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-78°C; 1 h;
参考文献
Cabezas, Jorge A.; Oehischlager, Allan C.
Tetrahedron Letters, 1995 , vol. 36, # 29 p. 5127 - 5130
反应条件
diisobutylaluminium hydride in hexane; dichloromethane T=-78°C;
参考文献
Chemical Communications, , vol. 46, # 23 p. 4178 - 4180
反应条件
Mn(OAc)3•2H2O; 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=22°C; 1 h;
参考文献
Organic Letters, , vol. 13, # 8 p. 2071 - 2073
反应条件
L-proline in tetrahydrofuran T=4°C; 14 h; Title compound not separated from byproducts;
参考文献
Cordova, Armando; Notz, Wolfgang; Barbas III, Carlos F.
Journal of Organic Chemistry, 2002 , vol. 67, # 1 p. 301 - 303
反应条件
piperidine; acetic acid 18 h;
参考文献
WO2003/95403 A1, ;
Page/Page column 4-6 ;
参考文献
Journal of the American Chemical Society, , vol. 71, p. 3471
反应条件
zinc(II) chloride in diethyl ether; water 1 h; Ambient temperature; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 58, # 9 p. 2517 - 2522
反应条件
morpholine; phosphoric acid T=90 - 95°C; 1 h;
参考文献
Furuhata, Akimichi; Onishi, Ken; Fujita, Akira; Kogami, Kunio
Agricultural and Biological Chemistry, 1982 , vol. 46, # 7 p. 1757 - 1760