(E,E)-2,4-己二烯醛合成路线 （共 87 条）
反应条件
sodium tetrahydroborate in water 2 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Furuhata, Akimichi; Onishi, Ken; Fujita, Akira; Kogami, Kunio
Agricultural and Biological Chemistry, 1982 , vol. 46, # 7 p. 1757 - 1760
反应条件
aluminum isopropoxide; isopropyl alcohol
参考文献
Fischer; Wiedemann
Justus Liebigs Annalen der Chemie, 1934 , vol. 513, p. 266,276
Justus Liebigs Annalen der Chemie, 1936 , vol. 522, p. 2,10
反应条件
in benzene Cyclization; 5 h; Irradiation;
参考文献
Oda, Kazuaki; Nakagami, Rikiji; Nishizono, Naozumi; Machida, Minoru
Chemical Communications, 1999 , # 23 p. 2371 - 2372
反应条件
1: iron; acetic acid; nickel acetate / unter Ausschluss von Luft, zuletzt auf dem Wasserbad View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 433, p. 126
反应条件
in tetrahydrofuran; diethyl ether T=-10°C; 1 h;
参考文献
Martelli, J.; Gree, D.; Kessabi, J.; Gree, R.; Toupet, L.
Tetrahedron, 1989 , vol. 45, # 13 p. 4213 - 4226
反应条件
in diethyl ether T=-78°C;
参考文献
Franck, Richard W.; Argade, S.; Subramaniam, C. S.; Frechet, Denise M.
Tetrahedron Letters, 1985 , vol. 26, # 27 p. 3187 - 3190
反应条件
1.1: MgClO4; H2SO4 / CHCl3 / 2 h / 25 °C 2.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -20 °C 2.2: n-BuLi / tetrahydrofuran; hexane / 2 h / -78 °C 3.1: 88 percent / imidazole / dimethylformamide / 3 h / 25 °C 4.1: 60 percent / (PCy)3Cl2Ru=CHPh(1,3-di-Mes-imidazolidine-2-yl) / CH2Cl2 / 2 h / 42 °C 5.1: mCPBA / CH2Cl2 / 0.08 h / -10 °C 5.2: Ac2O; Et3N / H2O; tetrahydrofuran / 12 h / 60 °C 6.1: 58 percent / NaHCO3 / methanol; H2O / 24 h 7.1: 58 percent / SO2Cl2 / diethyl ether / 0 °C View Scheme
参考文献
Garbaccio; Stachel; Baeschlin; Danishefsky
Journal of the American Chemical Society, 2001 , vol. 123, # 44 p. 10903 - 10908
反应条件
1: molecular sieve / pentane / 8 h / Ambient temperature 2: 1.) LDA / 1.) THF, -60 deg C, 16 h, 2.) THF, a) -60 deg C, 15 min, b) RT, 1 h View Scheme
参考文献
Bellassoued; Reboul; Salemkour
Synthetic Communications, 1995 , vol. 25, # 20 p. 3097 - 3108
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 3 h;
参考文献
Paquette,L.A.; Crouse,G.D.; Sharma,A.K.
Journal of the American Chemical Society, 1982 , vol. 104, p. 4411
反应条件
sodium tetrahydroborate in water 2 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Furuhata, Akimichi; Onishi, Ken; Fujita, Akira; Kogami, Kunio
Agricultural and Biological Chemistry, 1982 , vol. 46, # 7 p. 1757 - 1760
