(E,E)-2,4-己二烯醛合成路线 （共 87 条）
反应条件
1: NaBH4 / H2O / 2 h / Ambient temperature
2: 2.3 percent / H2 / (methyl benzoate)Cr(CO)6 / methanol / 2 h / 190 - 200 °C / 36775.4 Torr
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参考文献
Furuhata, Akimichi; Onishi, Ken; Fujita, Akira; Kogami, Kunio
Agricultural and Biological Chemistry, 1982 , vol. 46, # 7 p. 1757 - 1760
反应条件
1: isopropyl alcohol; aluminium isopropylate
2: pyridine
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参考文献
Reichstein; Ammann; Trivelli
Helvetica Chimica Acta, 1932 , vol. 15, p. 264
反应条件
2: 1.) lithium diisopropylamide, 2.) O2 / 1.) THF, hexane, -78 deg C, 45 min, 2.) a) -78 deg C -> room temperature, b) 2 h
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参考文献
Yang, Chau-Chen; Fang, Jim-Min
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 22 p. 3085 - 3094
参考文献
du Pont de Nemours and Co.
Patent: US2381880 , 1940 ;
Full Text Show Details
Kuhn; Hoffer
Chemische Berichte, 1930 , vol. 63, p. 2168
Chemische Berichte, 1931 , vol. 64, p. 1977
反应条件
ethanol; piperidinium acetate
T=20°C;
参考文献
Schmitt; Obermeit
Justus Liebigs Annalen der Chemie, 1941 , vol. 547, p. 291
参考文献
Schmitt; Obermeit
Justus Liebigs Annalen der Chemie, 1941 , vol. 547, p. 291
反应条件
in dichloromethane
0.5 h; Ambient temperature;
参考文献
Bestmann, Hans Juergen; Frey, Herbert
Liebigs Annalen der Chemie, 1980 , # 12 p. 2061 - 2071
