3,5-二甲基-1-金刚烷乙酸合成路线 (共 10 条)
反应条件
boron trifluoride diethyl etherate in sulfuric acid T=15°C;
参考文献
Lion, C.; Hedayatullah, M.; Bauer, P.; Boukou-Poba, J. P.; Charvy, C.; et al.
Bulletin des Societes Chimiques Belges, 1992 , vol. 101, # 3 p. 249 - 256
反应条件
sulfuric acid T=5 - 15°C; 1 h;
参考文献
Moiseev, I. K.; Stulin, N. V.; Yudashkin, A. V.; Klimochkin, Yu. N.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 7 p. 1655 - 1656,1472 - 1473
反应条件
sulfuric acid; nitric acid in chloroform T=42°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bull. Russ. Acad. Sci. Div. Chem. Sci. (Engl. Transl.), , vol. 41, # 7.2 p. 1612 - 1615,1244 - 1246
反应条件
1: aq. K2CO3 / 6 h / 150 °C 2: H2SO4, BF3 View Scheme
参考文献
Chemische Berichte, , vol. 101, p. 564 - 573
反应条件
sulfuric acid; boron trifluoride
参考文献
Chemische Berichte, , vol. 101, p. 564 - 573
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 38, # 10 p. 2947 - 2952
反应条件
1: (i) BF3, (ii) aq. KOH 2: (decarboxylation) View Scheme
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 38, # 10 p. 2947 - 2952
反应条件
(i) H2SO4, (ii) KMnO4, acetone; Multistep reaction;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 766, p. 51 - 57
反应条件
1: Br2 2: H2SO4 / 6 h / Heating 3: H2SO4, BF3 4: H2SO4 / 5 h / Heating View Scheme
参考文献
Bott,K.
Chemische Berichte, 1968 , vol. 101, p. 564 - 573
反应条件
lithium aluminium tetrahydride
参考文献
Landa; Burkhard; Vais
Collection of Czechoslovak Chemical Communications, 1973 , vol. 38, # 10 p. 2947 - 2952