反应条件
1.1: potassium tert-butylate / dimethyl sulfoxide / 0 - 20 °C / |Inert atmosphere 1.2: 4 h / 60 °C / |Inert atmosphere 2.1: dihydrogen peroxide / water; dichloromethane / 1.08 h / 20 °C / |Inert atmosphere; |Cooling with ice 3.1: tin(IV) chloride / dichloromethane / 12 h / -65 °C / |Inert atmosphere 4.1: diisobutylaluminium hydride / toluene / -78 - 0 °C / |Inert atmosphere View Scheme
参考文献
Zhu, Jia-Liang; Chen, Po-Erh; Huang, Hue-Wen
Tetrahedron Asymmetry, 2013 , vol. 24, # 1 p. 23 - 36