1-苯硫基-吡咯啉-2,5-二酮合成路线 (共 38 条)
反应条件
in hexane; 1,2-dichloro-ethane
参考文献
Reese, Colin Bernard
Patent: US2003/99981 A1, 2003 ;
反应条件
triethylamine in dichloromethane T=0 - 20°C; 18 h;
参考文献
Shimada, Hisashi; Kikuchi, Satoshi; Okuda, Saori; Haraguchi, Kazuhiro; Tanaka, Hiromichi
Tetrahedron, 2009 , vol. 65, # 31 p. 6008 - 6016
反应条件
N-chloro-succinimide; triethylamine in dichloromethane
参考文献
Merck and Co., Inc.
Patent: US5527819 A1, 1996 ;
反应条件
1: thiophenol With sulfuryl dichloride; triethylamine in dichloromethane T=0 - 20°C; 2: pyrrolidin-1-yl-2,5-dione With triethylamine in dichloromethane T=0 - 20°C; 1 h;
参考文献
Saravanan, Perumal; Anbarasan, Pazhamalai
Organic Letters, 2014 , vol. 16, # 3 p. 848 - 851
反应条件
in dichloromethane T=20°C; 24 h;
参考文献
Forbes, David C.; Bettigeri, Sampada V.; Al-Azzeh, Nahla N.; Finnigan, Brian P.; Kundukulam, Joseph A.
Tetrahedron Letters, 2009 , vol. 50, # 16 p. 1855 - 1857
反应条件
in dichloromethane 1 h;
参考文献
Harpp, David N.; Aida, T.; DeCesare, J.; Tisnes, P.; Chan, T. H.
Synthesis, 1984 , # 12 p. 1037
反应条件
tetrachloromethane; N-bromosuccinmide
参考文献
Groebel
Chemische Berichte, 1959 , vol. 92, p. 2887,2891
反应条件
pyridine; N-bromosuccinmide; benzene
参考文献
Miyoshi; Oda
Kogyo Kagaku Zasshi, 1956 , vol. 59, p. 224
Chem.Abstr., 1957 , p. 10413
参考文献
Groebel
Chemische Berichte, 1959 , vol. 92, p. 2887,2891
反应条件
boron trifluoride diethyl etherate in dichloromethane T=20 - 45°C; 4 h;
参考文献
Silvestri, Romano; De Martino, Gabriella; La Regina, Giuseppe; Artico, Marino; Massa, Silvio; Vargiu, Laura; Mura, Massimo; Loi, Anna Giulia; Marceddu, Tiziana; La Colla, Paolo
Journal of Medicinal Chemistry, 2003 , vol. 46, # 12 p. 2482 - 2493