2-叠氮乙基-2-乙酰氨基-2-脱氧-β-D-吡喃葡萄糖苷合成路线 （共 5 条）
反应条件
1: With sodium methylate in methanol T=20°C; 4 h; 2: in methanol
参考文献
Norberg, Oscar; Deng, Lingquan; Aastrup, Teodor; Yan, Mingdi; Ramstroem, Olof
Analytical Chemistry, 2011 , vol. 83, # 3 p. 1000 - 1007
反应条件
1.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve 1.2: 19 h / 20 °C 2.1: sodium methylate / methanol / 4 h / 20 °C 2.2: Amberlyst 15 View Scheme
参考文献
Wang, Wenjun; Jin, Chen; Guo, Lina; Liu, Yu; Wan, Yue; Wang, Xin; Li, Lei; Zhao, Wei; Wang, Peng George
Chemical Communications, 2011 , vol. 47, # 40 p. 11240 - 11242
反应条件
1: NaN3; tetrabutylammonium iodide / dimethylsulfoxide 2: NaOMe / methanol / 1 h / 20 °C View Scheme
参考文献
Park, Sungjin; Shin, Injae
Organic Letters, 2007 , vol. 9, # 9 p. 1675 - 1678
反应条件
1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / 50 °C 1.2: 0.17 h / 20 °C / Inert atmosphere 2.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve 2.2: 19 h / 20 °C 3.1: sodium methylate / methanol / 4 h / 20 °C 3.2: Amberlyst 15 View Scheme
参考文献
Wang, Wenjun; Jin, Chen; Guo, Lina; Liu, Yu; Wan, Yue; Wang, Xin; Li, Lei; Zhao, Wei; Wang, Peng George
Chemical Communications, 2011 , vol. 47, # 40 p. 11240 - 11242
反应条件
1: dichloromethane / 16 h / 20 °C 2: sodium methylate; methanol / 2 h / 0 °C View Scheme
参考文献
Adamiak, Kathrin; Anders, Thorsten; Henze, Manja; Keul, Helmut; Moeller, Martin; Elling, Lothar
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 84, p. 108 - 114
