1: With sec.-butyllithium in tetrahydrofuran; hexane
T=-78°C; Metallation; 1 h;
2: in tetrahydrofuran; hexane
T=-78 - 20°C; Rearrangement; Anionic ortho-Fries rearrangement; 12 h; Further stages.;
参考文献
Clayden, Jonathan; Helliwell, Madeleine; McCarthy, Catherine; Westlund, Neil
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 19 p. 3232 - 3249