2,3-二氢吡咯并[1,2-a]吲哚-1-酮合成路线 (共 7 条)
反应条件
oxygen; platinum (II) chloride in 1,2-dichloro-ethane P=760.051 Torr; 24 h; Heating;
参考文献
Li, Guotao; Huang, Xiaogen; Zhang, Liming
Angewandte Chemie - International Edition, 2008 , vol. 47, # 2 p. 346 - 349
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene T=100°C; Carbonylation; cyclization; P=60800 Torr; 3 h;
参考文献
Tetrahedron Letters, , vol. 40, # 40 p. 7153 - 7157
反应条件
acetic acid in water 12 h; Reflux;
参考文献
Derudas, Marco; Pala, Nicolino; Sanna, Vanna; Dallocchio, Roberto; Dessi, Alessandro; Roggio, Anna Maria; Sechi, Mario
Journal of Heterocyclic Chemistry, 2011 , vol. 48, # 5 p. 1161 - 1168
反应条件
1: 56 percent / aq. NaOH; n-Bu4NI 2: 94 percent / NaI / acetonitrile / 24 h / Heating 3: 39 percent / n-Bu3SnH; AIBN / benzene / 3 h / 100 °C / 60800 Torr View Scheme
参考文献
Tetrahedron Letters, , vol. 40, # 40 p. 7153 - 7157
反应条件
1: 94 percent / NaI / acetonitrile / 24 h / Heating 2: 39 percent / n-Bu3SnH; AIBN / benzene / 3 h / 100 °C / 60800 Torr View Scheme
参考文献
Tetrahedron Letters, , vol. 40, # 40 p. 7153 - 7157
反应条件
sodium hydride; acetic acid Yield given. Multistep reaction;
参考文献
Journal of Medicinal Chemistry, , vol. 39, # 26 p. 5035 - 5046
反应条件
1: sodium hydride / toluene; mineral oil / 5 h / Inert atmosphere; Reflux 2: acetic acid / water / 12 h / Reflux View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 48, # 5 p. 1161 - 1168