4-(1H-四唑-1-基)苯胺合成路线 （共 11 条）
反应条件
hydrogenchloride; tin(ll) chloride
参考文献
Chemische Berichte, , vol. 34, p. 3120
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in tetrahydrofuran; methanol T=20°C; 0.416667 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 48, # 12 p. 1947 - 1953
反应条件
1: With potassium carbonate in N,N-dimethyl-formamide T=70 - 75°C; 10 h; 2: With iron(III) chloride; carbon; hydrazine hydrate in tetrahydrofuran; methanol T=50°C; 10 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 48, # 12 p. 1935 - 1946
反应条件
1: 82 percent / K2CO3 / dimethylformamide / 32 h / 160 °C 2: 92 percent / N2H4*H2O; FeCl3; C* / methanol / 24 h / Heating 3: 68 percent / NaN3; AcOH / 4 h / 90 °C 4: H2; 6N aq. HCl / 10 percent Pd/C / methanol; tetrahydrofuran / 0.42 h / 20 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 48, # 12 p. 1947 - 1953
反应条件
1: 92 percent / N2H4*H2O; FeCl3; C* / methanol / 24 h / Heating 2: 68 percent / NaN3; AcOH / 4 h / 90 °C 3: H2; 6N aq. HCl / 10 percent Pd/C / methanol; tetrahydrofuran / 0.42 h / 20 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 48, # 12 p. 1947 - 1953
反应条件
1: 68 percent / NaN3; AcOH / 4 h / 90 °C 2: H2; 6N aq. HCl / 10 percent Pd/C / methanol; tetrahydrofuran / 0.42 h / 20 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 48, # 12 p. 1947 - 1953
反应条件
sodium hypophosphite; palladium on activated charcoal in water; toluene 2 h; Heating;
参考文献
Cristiano, M. Lurdes S.; Johnstone, Robert A. W.
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 3 p. 489 - 494
反应条件
1: 79 percent / HNO3 / 0.08 h / 100 °C 2: 0.15 g / sodium phosphinate / Pd-C / H2O; toluene / 2 h / Heating View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 3 p. 489 - 494
反应条件
hydrogenchloride in water
参考文献
Russian Journal of Organic Chemistry, , vol. 46, # 4 p. 556 - 560
反应条件
1: nitric acid 2: tin dichloride; fuming hydrochloric acid View Scheme
参考文献
Chemische Berichte, , vol. 34, p. 3120
