3-二氮杂-2-氧代丙酸乙酯合成路线 (共 20 条)
反应条件
1: 76 percent / diethyl ether / 5 °C 2: 68 percent / H2O, AcOH / ethanol / 6 h / Ambient temperature 3: 44 percent / tetrahydrofuran / Ambient temperature 4: 47 percent / ammonium acetate / acetic acid / 4 h / 90 °C View Scheme
参考文献
Ohsumi, Tadashi; Neunhoeffer, Hans
Tetrahedron, 1992 , vol. 48, # 25 p. 5227 - 5234
反应条件
boron trifluoride diethyl etherate in ethylene glycol dimethyl ether 3 h; Heating;
参考文献
Kim, Hong-Seok; Kwon, Il-Cheon; Kim, Oh-Hwoan
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 3 p. 937 - 940
反应条件
boron trifluoride diethyl etherate in ethylene glycol dimethyl ether 3 h; Heating;
参考文献
Kim, Hong-Seok; Kwon, Il-Cheon; Kim, Oh-Hwoan
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 3 p. 937 - 940
反应条件
Cu(acac)2 in benzene 4 h; Heating;
参考文献
Alonso, Miguel E.; Patricia, Jano
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 721 - 725
反应条件
diethyl ether; hydrogen bromide
参考文献
Ratusky; Sorm
Collection of Czechoslovak Chemical Communications, 1958 , vol. 23, p. 467,472
反应条件
diethyl ether; hydrogen bromide
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 23, p. 467,472
反应条件
boron trifluoride diethyl etherate in ethylene glycol dimethyl ether 3 h; Heating;
参考文献
Kim, Hong-Seok; Kwon, Il-Cheon; Kim, Oh-Hwoan
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 3 p. 937 - 940
反应条件
boron trifluoride diethyl etherate 3 h; Heating;
参考文献
Kim, Hong-Seok; Kwon, Il-Cheon; Kim, Oh-Hwoan
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 3 p. 937 - 940
反应条件
boron trifluoride diethyl etherate 3 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 32, # 3 p. 937 - 940
反应条件
boron trifluoride diethyl etherate in ethylene glycol dimethyl ether 3 h; Heating;
参考文献
Kim, Hong-Seok; Kwon, Il-Cheon; Kim, Oh-Hwoan
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 3 p. 937 - 940