1H-吡唑-3,5-二基二甲醇合成路线 （共 6 条）
反应条件
diisobutylaluminium hydride in toluene Reduction;
参考文献
Aran, Vicente J.; Kumar, Manoj; Molina, Jose; Lamarque, Laurent; Navarro, Pilar; Garcia-Espana, Enrique; Ramirez, Jose A.; Luis, Santiago V.; Escuder, Beatriz
Journal of Organic Chemistry, 1999 , vol. 64, # 17 p. 6135 - 6146
反应条件
1: 8.51 g / HCl / 24 h / 20 °C 2: 84 percent / DIBALH / toluene View Scheme
参考文献
Belda, Raquel; Pitarch-Jarque, Javier; Soriano, Conxa; Llinares, Jose M.; Blasco, Salvador; Ferrando-Soria, Jesus; Garcia-Espana, Enrique
Inorganic Chemistry, 2013 , vol. 52, # 19 p. 10795 - 10803
反应条件
1: KMnO4 / H2O / Heating 2: 8.51 g / HCl / 24 h / 20 °C 3: 84 percent / DIBALH / toluene View Scheme
参考文献
Aran, Vicente J.; Kumar, Manoj; Molina, Jose; Lamarque, Laurent; Navarro, Pilar; Garcia-Espana, Enrique; Ramirez, Jose A.; Luis, Santiago V.; Escuder, Beatriz
Journal of Organic Chemistry, 1999 , vol. 64, # 17 p. 6135 - 6146
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Olguin, Juan; Brooker, Sally
New Journal of Chemistry, 2011 , vol. 35, # 6 p. 1242 - 1253
反应条件
1: ammonium cerium (IV) nitrate; iodine / acetonitrile / Reflux 2: lithium aluminium tetrahydride / diethyl ether View Scheme
参考文献
Olguin, Juan; Brooker, Sally
New Journal of Chemistry, 2011 , vol. 35, # 6 p. 1242 - 1253
反应条件
1: dichloromethane 2: thionyl chloride View Scheme
参考文献
Belda, Raquel; Pitarch-Jarque, Javier; Soriano, Conxa; Llinares, Jose M.; Blasco, Salvador; Ferrando-Soria, Jesus; Garcia-Espana, Enrique
Inorganic Chemistry, 2013 , vol. 52, # 19 p. 10795 - 10803
