iron(II) bis(thiocyanate) in water; acetone T=-40 - -20°C;
参考文献
Grishchuk, B. D.; Gorbovoi, P. M.; Ganushchak, N. I.; Brush, D. M.; Kudrik, E. Ya.
Russian Journal of General Chemistry, 1993 , vol. 63, # 7.2 p. 1156 - 1158
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 7 p. 1655 - 1658
palladium diacetate in acetonitrile P=6619.6 Torr; 0.5 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 46, p. 4413 - 4416
N,N-methylenediacrylamide; Cu(BF4)2*6H2O in water; N,N-dimethyl-formamide byproducts: 3-MeC6H4CH2CH(SCN)CONHCH2NHCOCHCH2; addn. of 3-MeC6H4N2BF4 (1.1 equiv.) to N,N-methylenediacrylamide (1 equiv.) , Cu(BF4)2*6H2O (0.1 equiv.) and NH4SCN (1.1 equiv.) in H2O-DMF (1:3) for 30 min; evolution of gas at 10-15°C for 45 min;
参考文献
Grishchuk; Baranovskii; Gorbovoi; Ganushchak
Russian Journal of General Chemistry, 2003 , vol. 73, # 6 p. 957 - 960
