反应条件
Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '1697133', constants.ctx, '0')">1-n-pentyne</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1209227', constants.ctx, '0')">n-butyllithium</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a>; <a href="#" onclick="return RXDsubstances(event, this, '1730733', constants.ctx, '0')">hexane</a> <br />T=-78°C; 1 h; Inert atmosphere; <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '2088458', constants.ctx, '0')">2-phenylbenzyl bromide</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a>; <a href="#" onclick="return RXDsubstances(event, this, '1730733', constants.ctx, '0')">hexane</a> <br />T=-78 - 20°C; 19 h; Inert atmosphere; <br />
参考文献
Kwon, Yongseok; Cho, Hyunkyung; Kim, Sanghee Organic Letters, 2013 , vol. 15, # 4 p. 920 - 923