13-乙酰基-9-羟基巴卡丁III合成路线 （共 1 条）
反应条件
1: 75 percent / pyridine / 72 h / 23 °C 2: CrO3; aq. H2SO4 / acetone / 0.5 h / 23 °C 3: 20 percent / lithium tri-tert-butoxyaluminohydride / tetrahydrofuran / 0.5 h / 4 °C 4: 29 percent / 1,8-diazabicyclo[5,4,0]undec-7-ene / toluene / 1.5 h / 80 °C 5: 48 percent / NaBH4 / aq. phosphate buffer / 10 h / 23 °C / pH 7.0 View Scheme
参考文献
Nikolakakis, Anastasia; Caron, Gaetan; Cherestes, Alice; Sauriol, Francoise; Mamer, Orval; Zamir, Lolita O.
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 6 p. 1269 - 1280
