in dichloromethane byproducts: PPh3; mixt. of org. and Pd compds. in CH2Cl2 stirred for 2 d; concd. in vac., chromy. (silica-gel, hexane/EtOAc), solid dissolved in CH2Cl2, allowed stand at 0°C for 1 wk; elem. anal.;
参考文献
Zeitschrift fur Anorganische und Allgemeine Chemie, , vol. 630, # 8-9 p. 1177 - 1180
in benzene stirring of benzenic soln. (48 h/darkness/Ar atm.); pptn. of PdCl2*2PPh3;;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, # 10 p. 2174 - 2175
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 10 p. 2345 - 2346
tetrabutylammonium iodide in tetrahydrofuran byproducts: triphenylphosphine; to soln. of Pd-complex in THF was added B-complex in the presence of NBu4Cl, placed in NMR tube, 12 h, heated at 70°C for 3 h, PhI was added; detected by NMR;
参考文献
Marshall, William J.; Young Jr., Robert J.; Grushin, Vladimir V.
Organometallics, 2001 , vol. 20, # 3 p. 523 - 533
