反应条件
<b>Multi-step reaction with 2 steps<br /> </b>1.1: N-ethyl-N,N-diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / |Inert atmosphere<br />1.2: -78 - 20 °C / |Inert atmosphere<br />2.1: tetrakis(triphenylphosphine) palladium<sup>(0)</sup> / ethylene glycol dimethyl ether / 0.33 h / 80 °C / |Inert atmosphere; |Microwave irradiation<br /> <br />
参考文献
JANSSEN RandD IRELAND; GUILLEMONT, Jerôme, Emile, Georges; LANÇOIS, David, Francis, Alain; MOTTE, Magali, Madeleine, Simone; KOUL, Anil; BALEMANS, Wendy, Mia, Albert Patent: WO2013/21052 A1, 2013 ;
