1,2,4-苯三(羧酸乙基)酯合成路线 (共 14 条)
反应条件
copper dichloride; palladium dichloride in methanol; carbon dioxide T=40°C; P=120012 Torr; 12 h;
参考文献
Cheng, Jin-Sheng; Jiang, Huan-Feng
European Journal of Organic Chemistry, 2004 , # 3 p. 643 - 646
反应条件
phloroglucinol trimethyl ether; gold on TiO2 in 1,2-dichloro-benzene T=120°C; 0.5 h; Sealed tube; Catalytic behavior; ConcentrationReagent/catalyst;
参考文献
Abdulla, Khalid; Booth, Brian L.; Stacey, Catherine
Journal of Organometallic Chemistry, 1985 , vol. 293, p. 103 - 114
反应条件
Au nanoparticles/TiO2 (1 mol percent) in 1,2-dichloro-ethane T=65°C; 14 h; stereoselective reaction;
参考文献
Gryparis, Charis; Kidonakis, Marios; Stratakis, Manolis
Organic Letters, 2013 , vol. 15, # 23 p. 6038 - 6041
反应条件
tetra-N-butylammonium borohydride; zinc(II) iodide; CoBr2(1,2-bis(diphenylphosphino)ethane) in dichloromethane T=20°C; Cycloaddition; Diels-Alder reaction;
参考文献
Hilt; Du Mesnil
Tetrahedron Letters, 2000 , vol. 41, # 35 p. 6757 - 6761
反应条件
C23H22Cl2FeN4; zinc(II) iodide; zinc in acetonitrile T=50°C; 8 h; regioselective reaction;
参考文献
Liu, Yongbing; Yan, Xiaoyu; Yang, Nianfa; Xi, Chanjuan
Catalysis Communications, 2011 , vol. 12, # 6 p. 489 - 492
反应条件
oxygen; palladium dichloride in N,N-dimethyl-formamide P=3800.26 Torr;
参考文献
Jiang, Huan-Feng; Shen, Yan-Xia; Wang, Zhao-Yang
Tetrahedron Letters, 2007 , vol. 48, # 42 p. 7542 - 7545
反应条件
lt;CoH(N2)(PPh3)3gt; in acetonitrile T=22°C; 23 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Herrmann, Rudolf; Pombeiro, Armando J. L.
Monatshefte fuer Chemie, 1988 , vol. 119, p. 583 - 590
反应条件
in chloroform T=40°C; 117 h;
参考文献
Labuschagne, A. Johan H.; Malherbe, Johan S.; Meyer, Cornelius J.; Schneider, David F.
Synthetic Communications, 2002 , vol. 32, # 2 p. 297 - 304
反应条件
bulky-diarylamino-based PNP pincer ligand-Rh complex in benzene-d6 T=100°C; 24 h; Product distribution; Further Variations:Catalyststime;
参考文献
Weng, Wei; Guo, Chengyun; Celenligil-Cetin, Remle; Foxman, Bruce M.; Ozerov, Oleg V.
Chemical Communications, 2006 , # 2 p. 197 - 199
反应条件
bis(1,5-cyclooctadiene)nickel (0); triphenylphosphine T=-78 - 20°C; 18 h; Inert atmospherePressure vesselNeat (no solvent);
参考文献
Holte, Dane; Goetz, Daniel C. G.; Baran, Phil S.
Journal of Organic Chemistry, 2012 , vol. 77, # 2 p. 825 - 842