甲基 2-甲酰基-6-硝基苯甲酸合成路线 （共 4 条）
反应条件
4-methylmorpholine N-oxide in acetonitrile T=20°C; 20 h;
参考文献
Vu, Chi B.
Patent: US2013/190309 A1, 2013 ;
Location in patent: Paragraph 0393; 0394 ;
反应条件
1: potassium carbonate / butanone / 18 h / |Reflux 2: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / tetrachloromethane / 6 h / |Reflux 3: 4-methylmorpholine N-oxide / acetonitrile / 20 h / 20 °C View Scheme
参考文献
Vu, Chi B.
Patent: US2013/190309 A1, 2013 ;
反应条件
Pd-BaSO4; xylene Hydrogenation.Siedetemperatur;
参考文献
Eliel et al.
Journal of Organic Chemistry, 1953 , vol. 18, p. 1679,1682
反应条件
1: SOCl2 2: palladium/BaSO4; xylene / Hydrogenation.Siedetemperatur View Scheme
参考文献
Eliel et al.
Journal of Organic Chemistry, 1953 , vol. 18, p. 1679,1682
