4,4'-亚甲基二(1,2-苯二酚)合成路线 （共 11 条）
反应条件
boron tribromide in dichloromethane T=20°C; 4 h; Cooling with ice;
参考文献
Shi, Dayong; Li, Jing; Jiang, Bo; Guo, Shuju; Su, Hua; Wang, Tao
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 8 p. 2827 - 2832
反应条件
oxygen; ascorbic acid powder in water; acetonitrile T=20°C; pH=7; 24 h; Na-phosphate bufferEnzymatic reaction;
参考文献
Guazzaroni, Melissa; Crestini, Claudia; Saladino, Raffaele
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 1 p. 157 - 166
反应条件
boron tribromide in dichloromethane T=20°C;
参考文献
Oh, Ki-Bong; Lee, Ji Hye; Lee, Jong Wook; Yoon, Kyung-Mi; Chung, Soon-Chun; Jeon, Heung Bae; Shin, Jongheon; Lee, Hyi-Seung
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 3 p. 945 - 948
反应条件
1: polyphosphoric acid / 1 h / 80 °C 2: triethylsilane; trifluoroacetic acid / 20 °C 3: boron tribromide / dichloromethane / 4 h / 20 °C / Cooling with ice View Scheme
参考文献
Balaydin, Halis Tuerker; Durdagi, Serdar; Ekinci, Deniz; Sentuerk, Murat; Goeksu, Sueleyman; Menzek, Abdullah
Journal of Enzyme Inhibition and Medicinal Chemistry, 2012 , vol. 27, # 4 p. 467 - 475
反应条件
1: triethylsilane; trifluoroacetic acid / 20 °C 2: boron tribromide / dichloromethane / 4 h / 20 °C / Cooling with ice View Scheme
参考文献
Balaydin, Halis Tuerker; Durdagi, Serdar; Ekinci, Deniz; Sentuerk, Murat; Goeksu, Sueleyman; Menzek, Abdullah
Journal of Enzyme Inhibition and Medicinal Chemistry, 2012 , vol. 27, # 4 p. 467 - 475
反应条件
1: polyphosphoric acid / 1 h / 80 °C 2: triethylsilane; trifluoroacetic acid / 20 °C 3: boron tribromide / dichloromethane / 4 h / 20 °C / Cooling with ice View Scheme
参考文献
Balaydin, Halis Tuerker; Durdagi, Serdar; Ekinci, Deniz; Sentuerk, Murat; Goeksu, Sueleyman; Menzek, Abdullah
Journal of Enzyme Inhibition and Medicinal Chemistry, 2012 , vol. 27, # 4 p. 467 - 475
反应条件
hydrogenchloride; water
参考文献
Caro
Chemische Berichte, 1893 , vol. 26, p. 255
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Drabble; Nierenstein
Chemical Abstracts, 1907 , p. 1146
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Nierenstein; Webster
Chemische Berichte, 1908 , vol. 41, p. 81
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Silbermann; Ozorovitz
Chem. Zentralbl., 1908 , vol. 79, # II p. 1022
参考文献
Bischoff; Froehlich
Chemische Berichte, 1907 , vol. 40, p. 2781
Full Text Show Details
Caro
Chemische Berichte, 1893 , vol. 26, p. 255
Full Text Show Details
Drabble; Nierenstein
Chemical Abstracts, 1907 , p. 1146
Full Text Show Details
Nierenstein; Webster
Chemische Berichte, 1908 , vol. 41, p. 81
Full Text Show Details
Pougnet
Chem. Zentralbl., 1909 , vol. 80, # I p. 1508
Full Text Show Details
Silbermann; Ozorovitz
Chem. Zentralbl., 1908 , vol. 79, # II p. 1022
参考文献
Bischoff; Froehlich
Chemische Berichte, 1907 , vol. 40, p. 2781
Full Text Show Details
Caro
Chemische Berichte, 1893 , vol. 26, p. 255
Full Text Show Details
Drabble; Nierenstein
Chemical Abstracts, 1907 , p. 1146
Full Text Show Details
Nierenstein; Webster
Chemische Berichte, 1908 , vol. 41, p. 81
Full Text Show Details
Pougnet
Chem. Zentralbl., 1909 , vol. 80, # I p. 1508
Full Text Show Details
Silbermann; Ozorovitz
Chem. Zentralbl., 1908 , vol. 79, # II p. 1022
参考文献
Garofano; Oliverio
Annali di Chimica (Rome, Italy), 1957 , vol. 47, p. 896,904
Full Text Show Details
Arcoleo; Oliverio
Annali di Chimica (Rome, Italy), 1954 , vol. 44, p. 183,187
