N-(6-溴己基)氨基甲酸叔丁酯合成路线 （共 10 条）
反应条件
carbon tetrabromide; triphenylphosphine in toluene Ambient temperature;
参考文献
Keller; Haner
Helvetica Chimica Acta, 1993 , vol. 76, # 2 p. 884 - 892
反应条件
bromine; triethylamine in dichloromethane
反应条件
bromine; triethylamine in sodium hydroxide; dichloromethane; water
反应条件
1: BH3 / tetrahydrofuran / 1 h 2: Ph3P, CBr4 / tetrahydrofuran; acetonitrile / 24 h View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 37, # 16 p. 2537 - 2551
反应条件
1: 100 percent / aq. LiOH / tetrahydrofuran; ethanol / 20 °C 2: Et3N; diphenylphosphoryl azide / Heating 3: toluene / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 15 p. 4208 - 4212
反应条件
1: tetrahydrofuran / 1 h 2: TEA / CH2Cl2 / 2 h / 20 °C / cooling 3: LiBr / acetone; CH2Cl2 / 5 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2, , # 5 p. 923 - 927
反应条件
1: tetrahydrofuran / 1 h 2: TEA / CH2Cl2 / 2 h / 20 °C / cooling 3: LiBr / acetone; CH2Cl2 / 5 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2, , # 5 p. 923 - 927
反应条件
lithium bromide in dichloromethane; acetone 5 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 2, , # 5 p. 923 - 927
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 15 p. 4208 - 4212
反应条件
1: 86 percent / ethanol / 4 h / 45 °C 2: 69 percent / 3 M aq. HCl / ethyl acetate / 15 h / Ambient temperature View Scheme
参考文献
Keller; Haner
Helvetica Chimica Acta, 1993 , vol. 76, # 2 p. 884 - 892
