1: 1-n-pentyne With n-butyllithium in tetrahydrofuran; hexane T=0°C; 0.25 h; Inert atmosphere; 2: formic acid methyl ester in tetrahydrofuran; hexane T=0 - 20°C; 2.08333 h; Inert atmosphere;

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manganese(IV) oxide in dichloromethane T=20°C;