(三苯基膦)氯化金(I)合成路线 （共 181 条）
反应条件
in dimethyl sulfoxide for 45 min; not isolated, detected by NMR;
参考文献
Inorganic Chemistry, , vol. 45, # 13 p. 5201 - 5209
反应条件
in tetrahydrofuran under N2 atm. suspn. Ir and Au complexes in THF was stirred at room temp. for 6 h; soln. was concd., acetone was added and stirred for 10 min, ppt. was filtered and recrystd. from CHCl3-hexane;
参考文献
Khairul, Wan M.; Fox, Mark A.; Zaitseva, Natasha N.; Gaudio, Maryka; Yufit, Dmitry S.; Skelton, Brian W.; White, Allan H.; Howard, Judith A. K.; Bruce, Michael I.; Low, Paul J.
Dalton Transactions, 2009 , # 4 p. 610 - 620
反应条件
in not given at room temp.; not isolated, detected by NMR;
参考文献
Inorganic Chemistry, , vol. 45, # 13 p. 5201 - 5209
反应条件
in dichloromethane byproducts: 4-deuterobiphenyl; Irradiation (UV/VIS); under Ar, laser irradn. at 266 nm; monitored by UV and emission spectroscopy;
参考文献
Chemical Physics Letters, , vol. 436, # 1-3 p. 89 - 93
反应条件
in chloroform-d1 byproducts: (C6H5)3P(O)*HCl; AuCl3 and P(C6H5)3 were mixed in CDCl3; not sepd., detected by NMR spectra;
参考文献
Journal of Organometallic Chemistry, , vol. 694, # 4 p. 538 - 545
反应条件
in dichloromethane (N2); treatment of AuCl(C3H4N2Et2) with 1.5 equiv. of (C6H5CN)2PdCl2 in CH2Cl2 at ambient temp. in the presence of 1 equiv. of PPh3;
参考文献
Organometallics, , vol. 28, # 24 p. 6957 - 6962
反应条件
in chloroform-d1 byproducts: 2-(azidomethyl)phenyl isocyanide; under N2; in NMR tube; Au complex dissolved in CDCl3; treated with PPh3 (1 equiv.); not isolated; monitored by (31)P NMR spectra;
参考文献
Inorganica Chimica Acta, , vol. 356, p. 349 - 356
反应条件
in paraffin oil mulling in hot paraffin;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 1426 - 1430
反应条件
in dichloromethane stoich. amts. of educts stirred for 2 h, concd. in vac., ether added, filtered; filtrate evapd. to dryness, residue pptd. with methanol/water; recrystd. from methanol/water;
参考文献
Journal of Organometallic Chemistry, , vol. 221, # 2 p. 249 - 256
反应条件
in acetonitrile Irradiation (UV/VIS); irradiated at 254 nm with 100 W mercury lamp; monitored by UV;
参考文献
Inorganica Chimica Acta, , vol. 338, p. 105 - 110
