(三苯基膦)氯化金(I)合成路线 (共 181 条)
反应条件
in dichloromethane stoich. amts. of educts stirred for 2 h, concd. in vac., ether added, AuClPPh3 filtered; filtrate evapd. to dryness, residue pptd. with methanol/water; recrystd. from methanol/water;
参考文献
Journal of Organometallic Chemistry, , vol. 221, # 2 p. 249 - 256
参考文献
Inorganica Chimica Acta, , vol. 318, # 1-2 p. 38 - 44
反应条件
in dichloromethane Irradiation (UV/VIS); (under aerobic conditions); soln. of Au-complex in CH2Cl2 irradiated;
参考文献
Dalton Transactions, , # 17 p. 2248 - 2252
反应条件
in dichloromethane byproducts: Et4NClO4;
参考文献
Inorganica Chimica Acta, , vol. 37, p. 201 - 208
反应条件
in chloroform-d1 react. of equimolar mixt. under N2 at 30°C; not isolated, 31P-NMR;
参考文献
Polyhedron, , vol. 10, p. 1939 - 1950
反应条件
in benzene under N2 atm. mixt. Ru and Au complexes was heated in refluxed benzene; prep. TLC;
参考文献
Khairul, Wan M.; Fox, Mark A.; Zaitseva, Natasha N.; Gaudio, Maryka; Yufit, Dmitry S.; Skelton, Brian W.; White, Allan H.; Howard, Judith A. K.; Bruce, Michael I.; Low, Paul J.
Dalton Transactions, 2009 , # 4 p. 610 - 620
参考文献
Canadian Journal of Chemistry, , vol. 67, p. 1800 - 1806
反应条件
in dichloromethane color change from dark red to yellow, stirred (15 min); solvent removed (dark red residue), monitored by (31)P and (1)H NMR;
参考文献
Canadian Journal of Chemistry, , vol. 67, p. 1800 - 1806
反应条件
in not given monitored by (31)P NMR;
参考文献
Canadian Journal of Chemistry, , vol. 67, p. 1800 - 1806
反应条件
in methanol; chloroform-d1; dichloromethane Pt-complex in CDCl3 was reacted with Au-complex in MeOH and CH2Cl2, mixt. was stirred for 12 h, filtered off; monitored by NMR;
参考文献
Inorganica Chimica Acta, , vol. 312, # 1-2 p. 40 - 52