(三苯基膦)氯化金(I)合成路线 （共 181 条）
反应条件
hydrogenchloride in hydrogenchloride addn. of HCl to soln. of Au-complex, stirring (2 min); solvent removal (vac.), extn. of pentachlorophenol from solid residue by ether; ppt. dissoln. in chloroform, salting out by petroleum ether;
参考文献
Perevalova, E. G.; Smyslova, E. I.; Grandberg, K. I.; Struchkov, Yu. T.; Kuz'mina, L. G.; et al.
Sov. J. Coord. Chem. (Engl. Transl.), 1989 , vol. 15, p. 316 - 323
Koordinatsionnaya Khimiya, 1989 , vol. 15, p. 504 - 523
反应条件
hydrogenchloride in hydrogenchloride addn. of HCl to soln. of Au-complex, stirring (2 min); solvent removal (vac.), extn. of p-fluorophenol from solid residue by ether; ppt. dissoln. in chloroform, salting out by petroleum ether;
参考文献
Perevalova, E. G.; Smyslova, E. I.; Grandberg, K. I.; Struchkov, Yu. T.; Kuz'mina, L. G.; et al.
Sov. J. Coord. Chem. (Engl. Transl.), 1989 , vol. 15, p. 316 - 323
Koordinatsionnaya Khimiya, 1989 , vol. 15, p. 504 - 523
反应条件
hydrogenchloride in hydrogenchloride addn. of 0.1 N HCl to soln. of Au-complex, stirring (2 min); solvent removal (vac.), extn. of chlorophenol from solid residue by ether; ppt. dissoln. in chloroform, salting out by petroleum ether;
参考文献
Perevalova, E. G.; Smyslova, E. I.; Grandberg, K. I.; Struchkov, Yu. T.; Kuz'mina, L. G.; et al.
Sov. J. Coord. Chem. (Engl. Transl.), 1989 , vol. 15, p. 316 - 323
Koordinatsionnaya Khimiya, 1989 , vol. 15, p. 504 - 523
反应条件
hydrogenchloride in hydrogenchloride addn. of HCl to soln. of Au-complex, stirring (2 min); solvent removal (vac.), extn. of p-fluorophenol from solid residue by ether; ppt. dissoln. in chloroform, salting out by petroleum ether;
参考文献
Perevalova, E. G.; Smyslova, E. I.; Grandberg, K. I.; Struchkov, Yu. T.; Kuz'mina, L. G.; et al.
Sov. J. Coord. Chem. (Engl. Transl.), 1989 , vol. 15, p. 316 - 323
Koordinatsionnaya Khimiya, 1989 , vol. 15, p. 504 - 523
反应条件
hydrogenchloride in hydrogenchloride addn. of HCl to soln. of Au-complex, stirring (2 min); solvent removal (vac.), extn. of o-bromophenol from solid residue by ether; ppt. dissoln. in chloroform, salting out by petroleum ether;
参考文献
Perevalova, E. G.; Smyslova, E. I.; Grandberg, K. I.; Struchkov, Yu. T.; Kuz'mina, L. G.; et al.
Sov. J. Coord. Chem. (Engl. Transl.), 1989 , vol. 15, p. 316 - 323
Koordinatsionnaya Khimiya, 1989 , vol. 15, p. 504 - 523
反应条件
hydrogenchloride in hydrogenchloride addn. of HCl to soln. of Au-complex, stirring (2 min); solvent removal (vac.), extn. of p-cresol from solid residue by ether; ppt. dissoln. in chloroform, salting out by petroleum ether;
参考文献
Perevalova, E. G.; Smyslova, E. I.; Grandberg, K. I.; Struchkov, Yu. T.; Kuz'mina, L. G.; et al.
Sov. J. Coord. Chem. (Engl. Transl.), 1989 , vol. 15, p. 316 - 323
Koordinatsionnaya Khimiya, 1989 , vol. 15, p. 504 - 523
反应条件
hydrogenchloride in hydrogenchloride addn. of 0.1 N HCl to soln. of Au-complex, stirring (2 min); solvent removal (vac.), extn. of pyrocatechol from solid residue by ether; ppt. dissoln. in chloroform, salting out by petroleum ether;
参考文献
Perevalova, E. G.; Smyslova, E. I.; Grandberg, K. I.; Struchkov, Yu. T.; Kuz'mina, L. G.; et al.
Sov. J. Coord. Chem. (Engl. Transl.), 1989 , vol. 15, p. 316 - 323
Koordinatsionnaya Khimiya, 1989 , vol. 15, p. 504 - 523
反应条件
hydrogenchloride in hydrogenchloride addn. of 0.1 N HCl to soln. of Au-complex, stirring (2 min); solvent removal (vac.), extn. of pentafluorophenol from solid residue by ether; ppt. dissoln. in chloroform, salting out by petroleum ether;
参考文献
Perevalova, E. G.; Smyslova, E. I.; Grandberg, K. I.; Struchkov, Yu. T.; Kuz'mina, L. G.; et al.
Sov. J. Coord. Chem. (Engl. Transl.), 1989 , vol. 15, p. 316 - 323
Koordinatsionnaya Khimiya, 1989 , vol. 15, p. 504 - 523
反应条件
in dichloromethane stirring of stoich. amts. (room temp., 30 min); filtration (Celite), concn., crystn. on Et2O diffusion to soln.;
参考文献
Chan, Chi-Keung; Guo, Chun-Xiao; Cheung, Kung-Kai; Li, Dan; Che, Chi-Ming
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1994 , # 24 p. 3677 - 3682
反应条件
in diethyl ether addn. of Au complex to Tl compd. suspension under N2, room temp.; stirring, 3h, room temp.; filtering off pptd. Au complex; evapn. to a small volume; add. of hexane; pptn.; elem. anal.;
参考文献
Fernandez, Eduardo J.; Jones, Peter G.; Laguna, Antonio; Mendia, Aranzazu
Inorganica Chimica Acta, 1994 , vol. 215, p. 229 - 234
