反应条件
1.1: n-butyllithium / hexane; tetrahydrofuran / 0.58 h / -40 °C / |Inert atmosphere
1.2: 1.25 h / -40 - 20 °C / |Inert atmosphere
2.1: gold(I) chloride / toluene / 11.5 h / 20 °C / |Schlenk technique; |Inert atmosphere
3.1: potassium tert-butylate; oxygen / tetrahydrofuran; dimethyl sulfoxide / 26 h / 20 °C / 760.05 Torr
View Scheme
参考文献
Qiu, Youai; Ma, Dengke; Fu, Chunling; Ma, Shengming
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 10 p. 1666 - 1671
