反应条件
1: 5 palladium on charcoal; hydrogen / N,N-dimethyl acetamide; dichloromethane; hexan-1-ol / 45 °C / 258.58 Torr / |Inert atmosphere
2: hydrogenchloride; sodium nitrite / N,N-dimethyl acetamide; dichloromethane; hexan-1-ol; water / 0.02 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Chen, Mao; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 15 p. 4247 - 4250
Angew. Chem., 2013 , vol. 125, # 15 p. 4341 - 4344,4
