反应条件
1.1: oxygen; palladium (II) trifluoroacetate; benzoic acid / 24 h / 120 °C / |Schlenk technique
2.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 2 h / -40 - 20 °C
2.2: 5 h / 20 °C
3.1: pyridine; trimethylsilyl iodide / sulfolane / 20 h / 70 °C / |Inert atmosphere
4.1: anhydrous iron chloride; tert.-butylhydroperoxide; pyridine-2,6-dicarboxylate N-oxide / water; 1,1-dimethylpropan-1-ol / 8 h / 20 °C / |Cooling with ice
View Scheme
参考文献
Ramkumar, Nagarajan; Nagarajan, Rajagopal
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2802 - 2807