triethylamine T=20°C; 18 h;

lithium chloride or (C2H5)3CH2C6H5NCl or n-C4H9NBr in butan-1-ol Electrolysis; (N2 or Ar); using of Sn as anode and stainless steel plate as cathode; electrolysis for 1-1.5 h with soln. of electrolyte LiCl, Bu4NBr or Et3BzNC in n-butanol; sepn. from electrolyte, washing with absolute alcohol; drying in vac.; elem. anal.;

in toluene an excess of n-butanol was aded to a soln. of Sn(OCH3)2 in toluene; Gsell, R.; Zeldin, M. J. Inorg. Nucl. Chem. 1975,37,1133;