反应条件
1.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C / Inert atmosphere 1.2: 3 h / -78 - -30 °C / Inert atmosphere 2.1: lithium diisopropyl amide / tetrahydrofuran / Inert atmosphere; Cooling 2.2: Inert atmosphere; Cooling 3.1: 1,1-dimethylethylmagnesium chloride / tetrahydrofuran / -45 °C / Inert atmosphere 3.2: -45 - 20 °C / Inert atmosphere View Scheme
参考文献
Fukuda, Shigehiko; Tsuji, Kazuhito; Musashi, Jun; Nonaka, Ryo; Kimura, Tsutomu; Satoh, Tsuyoshi
Synthesis, 2011 , # 22 art. no. F71511SS, p. 3615 - 3626
