[2,4]-二苯并-18-冠醚-6合成路线 （共 5 条）
反应条件
potassium hydroxide in dimethyl sulfoxide T=90°C; 2.5 h;
参考文献
Kotlyar; Gorodnyuk; Grigorash; Chuprin
Russian Journal of General Chemistry, 1998 , vol. 68, # 7 p. 1135 - 1138
反应条件
1: 2,2'-lt;1,2-ethanediylbis(oxy-2,1-ethanediyloxy)gt;bisphenol With caesium carbonate in acetonitrile 3 h; RefluxInert atmosphere; 2: diethylene glycol dimethanesulfonate in acetonitrile Inert atmosphereReflux;
参考文献
Hanes, Robert E.; Lee, Jong Chan; Ivy, Sheryl N.; Palka, Anna; Bartsch, Richard A.
Arkivoc, 2010 , vol. 2010, # 7 p. 238 - 248
反应条件
1: 2,2'-lt;1,2-ethanediylbis(oxy)gt;bisphenol With caesium carbonate in acetonitrile 3 h; RefluxInert atmosphere; 2: triethyleneglycol bismethanesulfonyl ester in acetonitrile Inert atmosphereReflux;
参考文献
Hanes, Robert E.; Lee, Jong Chan; Ivy, Sheryl N.; Palka, Anna; Bartsch, Richard A.
Arkivoc, 2010 , vol. 2010, # 7 p. 238 - 248
反应条件
potassium hydroxide in ethanol; N,N-dimethyl-formamide; butan-1-ol Heating;
参考文献
Weber, Edwin
Chemische Berichte, 1985 , vol. 118, # 11 p. 4439 - 4452
反应条件
potassium hydroxide 1) isoamyl alcohol, boiled , water trap, 2) 10 h, boiled; Yield given. Multistep reaction;
参考文献
Gorodnyuk, V. P.; Ivanov, O. V.; Kotlyar, S. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 12 p. 1414 - 1415
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , # 12 p. 1697 - 1698
