4,4'-二壬基-2,2'-联吡啶合成路线 (共 2 条)
反应条件
n-butyllithium; diisopropylamine in tetrahydrofuran T=0 - 20°C; 15 h; Inert atmosphere;
参考文献
Neuthe, Katja; Bittner, Florian; Stiemke, Frank; Ziem, Benjamin; Du, Juan; Zellner, Monika; Wark, Michael; Schubert, Thomas; Haag, Rainer
Dyes and Pigments, 2014 , vol. 104, p. 24 - 33
反应条件
1: 11 percent / Raney Ni / 60 h / Heating 2: 1.) LDA / 1.) THF, 0 deg C, 3 h, 2.) THF, 0 deg C, 3 h View Scheme
参考文献
Journal of the American Chemical Society, , vol. 120, # 2 p. 305 - 316