甲基3,5-二碘苯甲酸酯合成路线 （共 11 条）
反应条件
tetrahydrofuran; isopentyl nitrite
参考文献
Li, Feirong; Yang, Sung Ik; Ciringh, Yangzhen; Seth, Jyoti; Martin II, Charles H.; Singh, Deepak L.; Kim, Dongho; Birge, Robert R.; Bocian, David F.; Holten, Dewey; Lindsey, Jonathan S.
Journal of the American Chemical Society, 1998 , vol. 120, # 39 p. 10001 - 10017
反应条件
sulfuric acid 7.5 h; Reflux;
参考文献
GEORGIA TECH RESEARCH CORPORATION; ZUNIGA, Carlos; MARDER, Seth; HASKE, Wojciech; KIPPELEN, Bernard; FENG, Daijun
Patent: WO2014/11491 A1, 2014 ;
Location in patent: Page/Page column 19 ;
反应条件
in methanol 7.5 h; Reflux;
参考文献
Georgia Tech Research Corporation; SOLVAY (Societe Anonyme)
Patent: WO2009/80799 A2, 2009 ;
Location in patent: Page/Page column 57-58 ;
反应条件
CH3SO3H in methanol; water; ethyl acetate
参考文献
GEORGIA TECH RESEARCH CORPORATION
Patent: US2010/331509 A1, 2010 ;
反应条件
1: 60 percent / ICl / CH2Cl2 2: 71 percent / isopentyl nitrite, THF View Scheme
参考文献
GEORGIA TECH RESEARCH CORPORATION; HE, Xuyang; ZHANG, Yadong; MARDER, Seth; HASKE, Wojciech; KIPPELEN, Bernard
Patent: WO2014/11477 A1, 2014 ;
反应条件
potassium carbonate in acetone 8 h; Heating;
参考文献
Endres, Andreas; Maas, Gerhard
Tetrahedron, 2002 , vol. 58, # 20 p. 3999 - 4005
反应条件
1: H2SO4 2: 71 percent / isopentyl nitrite, THF View Scheme
参考文献
Li, Feirong; Yang, Sung Ik; Ciringh, Yangzhen; Seth, Jyoti; Martin II, Charles H.; Singh, Deepak L.; Kim, Dongho; Birge, Robert R.; Bocian, David F.; Holten, Dewey; Lindsey, Jonathan S.
Journal of the American Chemical Society, 1998 , vol. 120, # 39 p. 10001 - 10017
反应条件
1.1: NaNO2; aq. sulfuric acid / 2 h 1.2: 82 percent / urea; aq. KI / 5 h / 20 °C 2.1: 82 percent / K2CO3 / acetone / 8 h / Heating View Scheme
参考文献
Endres, Andreas; Maas, Gerhard
Tetrahedron, 2002 , vol. 58, # 20 p. 3999 - 4005
反应条件
diisobutylaluminium hydride in tetrahydrofuran; dichloromethane T=0°C; 4 h; Inert atmosphere;
参考文献
Zhou, Ningzhang; Zhao, Yuming
Journal of Organic Chemistry, 2010 , vol. 75, # 5 p. 1498 - 1516
反应条件
diisobutylaluminium hydride; pyridinium chlorochromate Yield given. Multistep reaction;
参考文献
Li, Feirong; Yang, Sung Ik; Ciringh, Yangzhen; Seth, Jyoti; Martin II, Charles H.; Singh, Deepak L.; Kim, Dongho; Birge, Robert R.; Bocian, David F.; Holten, Dewey; Lindsey, Jonathan S.
Journal of the American Chemical Society, 1998 , vol. 120, # 39 p. 10001 - 10017
