反应条件
1: oxalyl chloride / 0.5 h / Ambient temperature
2: N-hydroxypyridine-2-thione sodium salt, 4-dimethylaminopyridine, bromotrichloromethane / CCl4 / 0.25 h / Heating
3: 73 percent / lithium aluminium hydride / tetrahydrofuran / Heating
View Scheme
参考文献
Beckwith, A. L. J.; Raner, K. D.
Journal of Organic Chemistry, 1992 , vol. 57, p. 4954 - 4962