4-(3’,6’-二甲基-3’-庚基)苯酚合成路线 （共 5 条）
反应条件
boron tribromide in dichloromethane T=0°C; 1.5 h;
参考文献
Lalah, Joseph O.; Schramm, Karl-W.; Lenoir, Dieter; Henkelmann, Bernhard; Hertkorn, Norbert; Matuschek, Georg; Kettrup, Antonius; Guenther, Klaus
Chemistry - A European Journal, 2001 , vol. 7, # 22 p. 4790 - 4795
反应条件
boron trifluoride diethyl etherate in Petroleum ether T=50°C; Friedel-Crafts alkylation; 0.25 h;
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 45, # 14 p. 1253 - 1263
反应条件
1: aq. HBr / 1 h / Heating 2: 90.6 mg / AlCl3 / hexane / 20 °C 3: 70.2 mg / BBr3 / CH2Cl2 / 1.5 h / 0 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 7, # 22 p. 4790 - 4795
反应条件
1: 90.6 mg / AlCl3 / hexane / 20 °C 2: 70.2 mg / BBr3 / CH2Cl2 / 1.5 h / 0 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 7, # 22 p. 4790 - 4795
反应条件
1.1: Mg / diethyl ether / 0.5 h / Heating 1.2: 68.4 percent / diethyl ether / 2 h / Heating 2.1: aq. HBr / 1 h / Heating 3.1: 90.6 mg / AlCl3 / hexane / 20 °C 4.1: 70.2 mg / BBr3 / CH2Cl2 / 1.5 h / 0 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 7, # 22 p. 4790 - 4795
