反式-1,2-双(三丁基锡)乙烯合成路线 (共 5 条)
反应条件
dichloro bis(acetonitrile) palladium(II); N-ethyl-N,N-diisopropylamine in tetrahydrofuran; N,N-dimethyl-formamide T=25°C; 24 h; Yield given;
参考文献
Nicolaou; Chakraborty; Piscopio; Minowa; Bertinato
Journal of the American Chemical Society, 1993 , vol. 115, # 10 p. 4419 - 4420
反应条件
N-ethyl-N,N-diisopropylamine; lt;Pd(CH3CN)Cl2gt; in tetrahydrofuran; N,N-dimethyl-formamide T=25°C; 48 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Nicolaou, K. C.; Piscopio, Anthony D.; Bertinato, Peter; Chakraborty, Tushar K.; Minowa, Nobuto; Koide, Kazunori
Chemistry--A European Journal, 1995 , vol. 1, # 5 p. 318 - 333
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane Heatingother times, other stannanes, other acid chlorides; palladium-catalyzed coupling of acid chlorides with stannanes;
参考文献
Echavarren, Antonio M.; Perez, Marta; Castano, Ana M.; Cuerva, Juan M.
Journal of Organic Chemistry, 1994 , vol. 59, # 15 p. 4179 - 4185
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=60°C; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 59, # 15 p. 4179 - 4185
反应条件
Yield given. Multistep reaction;
参考文献
Peel, Michael R.; Johnson, Carl R.
Tetrahedron Letters, 1986 , vol. 27, # 49 p. 5947 - 5950