manganese(IV) oxide in tetrahydrofuran T=40°C; 1 h;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '11460447', constants.ctx, '0')">lithium aluminium tetrahydride</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />T=0 - 5&deg;C;&nbsp;1&nbsp;h;&nbsp;<br /> <br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: trichlorophosphate; N,N-diethylaniline / 105 &deg;C<br />2: triethylamine / dichloromethane; tetrahydrofuran / 3 h / -78 &deg;C<br />3: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 5 &deg;C<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: triethylamine / dichloromethane; tetrahydrofuran / 3 h / -78 &deg;C<br />2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 5 &deg;C<br /> <br /> &nbsp;